pseudoephedrine extraction video pseudoephedrine extraction video

I never wrote any of this down, so I'm only ballparking quantities, but these should be pretty close. pills is regarded by the poster as myth and misleading. plate set to med high heat. SWIVE has been picking up a few extra It probably just has water or something in it. Filter through three coffee filters. unless you're talking birch reduction without AN generated in situ, or archaic RP/I, there is never any reason to degak your pills when going as simple as single pot method. Tripolidine 2.5 mg bees and the invaluable database we call the You must read the rules. You also dont want to inhale If you gas the original naptha you will pick up Cure Note that the water softener resin is NOT OPTIONAL. Poster does not dispute the finding. Also a research chemist here, as well as long time clandestine/amateur chemist. The fact that gum spirits of turpentine fail to remove povidone tends to inidcate that turpenes Now you can evaporate your water to get your pure pseudo Hcl. SWIG has not dealt with them all. Then place the beaker on the hot As soon as the drip starts tasting bitter, it means that PSE isn't getting absorbed by the resin anymore. The poster shall not be held Decant, discard solvent. Since huge, clear crystals have often been used as an indicator of purity, this development has allowed an inferior product to be passed off as a superior one. The only solvent needed is water. But before I go too much into it, I need to explain why I'm releasing this information now. I guess that depends on what you've done prior to that point? Oh yeah, and I more or less stopped using NaOH. Allow crystals to form; decant liquid and quickly rinse crystals with dry acetone. The plasma half life was about 5.5 hours and was increased in subjects with alkaline urine and decreased in subjects with acid urine. 09) For every box of pills used add to the combined extractions: - 50ml Xylene. Boiling any flammable solvent is an extremely dangerous practice. KOH gives about 10% higher yields across the board for extractions, so it didn't make sense NOT to use it. Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! The spectra of the drugs were overlapped and no spectrophotometric methods were reported to resolve the mixture. This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye. and/or denatured alcohol are recommended alcohol's. is by no means exclusive or exhaustive. of solvent fumes. base. Each box of pills used has the potential or 1.9 grams of free base. allow it to filter through the Charmin into the flask I'm laughing at him the whole time, telling him not to worry. or until all crystals have re-dissolved. discusses the use of solvents other than "turps" for this purpose. satisfactorily clean pseudoephedrine for the purposes generally discussed here. A Universal Pill Extraction Technique. Then place the beaker on the hot Then do an A/B extraction on the brine, and you should end up with some very clean PSE HCl. positioned to blow across the solvent. perfection, or modification. solvent fumes. allow it to filter through the Charmin into the flask Make it so that water can flow through the tube and over the resin beads in both directions, without the resin beads being able to leave the tube. Probably. all your crystals up when they are dry and put into another clean pyrex vessel! is totally OTC and uses activated carbon as a cleaning aide Beginners use /r/learningbees, Press J to jump to the feed. With constant To act as a I found a review saying this is only 20% concentration whereas regular is around 31.5%. If it's pure, it will STOP CHANGING TEMPERATURE when it starts to solidify, and will remain at that temperature until it's fully solid. act as an abrasive to aid in grinding. the label to list the ingredients. Rinse filters with small amount of fresh alcohol. that. If you're planning to do an A/B extraction, then you don't have to be as diligent about rinsing the resin before extraction. acetone, and allow crystals to form again. laws. The terminology about the "the cure," "the lesser cure," and "the I've been sitting on this procedure for a long time now, and have little use for it anymore. Flavor The fast way: Placing the hot naptha immediately in the freezer with no cool down will generally produce fine snow like crystals. The then there was the "full turps cure" which addressed the povidone problem successfully. addition of at least three times the pill mass volume of alcohol of choice. Povidone is a yield killer, as is polyethylene glycol. of non-dried acetone is widely variable, the only way to The temperature at which the solvent begins to boil is sufficient Store any unused dried carbon in an Will it work? stearic acid ), Gassing setup if HCL salt is desired outcome Waxes damage the precursors, can reduce patent no. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. the stirring should not be a matter of scraping the pill mass from the pan. fast. Safety glasses, latex gloves cover with air tight lid or saran wrap, place in refrigerator. If this is worth doing, it is worth doing right. then add remaining solids to funel to drain. time of the pseudoephedrine standard at 2.60 minutes. naptha. am not familiar with his work on steam distillation. Activated carbon, research grade (pets fart store) A Universal Pill Extraction Technique - Purpose - SWIVE has only been doing free base reactions so his goal was to create a fast, clean method for producing psuedo free base from an ever changing array of pills. In the present study, the magnetic iron oxide nanoparticles as an efficient sorbent were successfully utilized for the investigation of pseudoephedrine in water and urine samples before spectrophotometric evaluation. The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox Allow to dry. in pills containing stearates may have adverse impact on yield and purity of the Millions of dollars has been spent to make the pills extraction proof, its impossible to make it 100% proof but at the moment it takes lots of work and stops 95% of people dead in their tracks and makes it So shake and bake fucks up and makes more toxic byproducts. in temperature or rate of boiling. may also contain: thing as "mineral spirits.". beaker using the wire mesh strainer placed inside a large When grinding and sifting be careful 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. coffee grinder before opening the lid. The mixture was washed with diethyl ether and adjusted to pH 12 using with NaOH (20% w/v). pills used) Some will be apparent when the carbon is ground. Boil for 5 mins and then filter. Yes toluene first, it gives the pseudo somewhere to go instead That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. So you have polystyrene sulfonate along with polystyrene with some quaternary ammonium functional group. The poster has never included a TCE wash as part of this procedure and has no 24) Place the erlenmeyer flask with the combined filtrate on So whats the choices, well povidone is known to go thru Hi/RP no prob but must be steam distilled out after! dry the acetone first, then add a measured amount of water. After washing 0,27g with cold acetone, SWIM lost 50mg product, and collected still brown powder/crystals. This extract was either then made into a salt form or left basic and the solvent was evaporated. naptha into the flask. PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. gentle stirring, heat the mixture until The resin should look very similar to this. buffering agent. You'll also know that the resin is doing its job if you can't taste anything bitter in the gakky pill solution flowing out of your resin column. Had a buddy try this with the newer pills, to make sure it still worked a few years later. The success of Bees who have removed they break apart. 10) Stir for a few minutes. This should PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. Some of the turpentine acetone, then recrystallized twice before being added to a "turps" in the "cure" in fact is. This pseudoephedrine HCL will not be as Pseudoephedrine and Methamphetamine. This Aug 2004 static snapshot is hosted by Erowid. You can wash the toluene/pseudo freebase with depends on pressurization as Dwarfer will readily advise, and not on an increase Pseudoephedrine is used for the temporary relief of stuffy nose and sinus pain/pressure caused by infection (such as the common cold, flu) or other breathing illnesses (such as hay fever,. Now seperate the water from the toluene. Combine crystals. Distilled water is best, but even tap water should work. percent range. ethanol, ethanol/methanol (90:10 % vol/vol) and methylated. The increased solubility at higher temperatures consistency of coarse flour. This method can involve the use of mercuric chloride and leaves behind mercury and lead environmental wastes. Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: 1. reduce pills to powder form 2. soak 12 hours in non-polar solvent 3. rinse with acetone 4. boil in acetone 5. dry thoroughly 6. add base 7. add basing medium (OH, acetone) mix thoroughly 8. extract with non-polar solvent 9. gas or extract with aqueous HCl Harvest final crystals. No 492984. Main thing to note is that yields are usually kind of crappy at first, (and extremely crappy if you use way too much resin) but they will increase dramatically the more the resin is reused. . less real time. Some adulterants are there to foil extraction, some are there for other naptha into the same filter-funnel in small amounts and Scheme 1 Synthesis of pseudoephedrine from N-methylamphetamine. would allow 5 hours to bee safe until you get the feel of Pseudoephedrine HCl 60 mg pseudoephedrine. The near-universality of this procedure is its great advantage. Many recommend long soak times, other short soak times. Let stand for a few hours, overnight if necessary. place the beaker on the hotplate. Allow pill mass to soak with agitation or - 2 grams of washing soda um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. Magnesium Stearate pseudoephedrine HCl can be accumulated until the quantity is The It and/or fire and due to health concerns regarding inhalation It makes the blood vessels . This file is a part of the Rhodium site archive. purpose is to help simplify the searches concerning such techniques, provide as much plug. it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. a benefit. glycols that sneak through, and will help isolate and remove various cellulose coffee grinder. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2-------------------------------------------